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Cyclic voltammograms for (A) phenPS (0.4 mM) and (B) naphPS (0.4 mM) in the presence of [Cu(I)(CH3CN)4]BF4 (0.2 mM) in methanol at 25°C (0.1 M Bu4NPF6, glassy carbon electrode, 100 mV/s scan rate, Ag+/Ag reference electrode with Fc+/Fc as external reference).