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. Author manuscript; available in PMC: 2020 Oct 21.
Published in final edited form as: Inorg Chem. 2019 May 24;58(20):13631–13638. doi: 10.1021/acs.inorgchem.9b00965

TABLE 1.

Selected bond distances (Å) and angles (deg) describing the ligand geometry in the crystal structures of phenPS•CH2Cl2 (5) and naphPS• 3CH2Cl2 (7).

Parameter 5 7
P(1)-C(1) 1.8568(5) 1.8616(12)
P(1)-C(4) 1.8544(6) 1.8614(13)
P(1)-C(7) 1.8442(5) 1.8514(12)
P(1)•••P(1)’ 3.0703(5) 2.9552(6)
P(1)-C(7)-C(12) 116.715(16) 121.84(9)
P(1)-C(1)-P(2) 108.20(3) 114.68(6)
C(1)-P(2)-S(1) 111.686(19) 114.74(4)
P(1)-C(7)•••C(7)’-P(1)’ 3.66(9) 21.76(9)