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Analysis of the synthesized nucleotide sugars compounds 3 and 6 by capillary electrophoresis with UV detection (CE-UV) and electrospray ionization mass spectrometry (ESI-MS).
| Compound | Amount [µmol] | Average Yield [%] | Calculated m/z [M − H]− | Observed m/z [M − H]− |
|---|---|---|---|---|
| 3 (UDP-[15N]GlcNAc) | 200 | 100% | 607.1 (a) | 607.2 |
| 6 (UDP-[13C6]Gal) | 400 | 100% | 571.3 (a) | 570.9 |
| UDP-GlcNAc (a) | 606.1 | 606.2 | ||
| UDP-Gal (a) | 565.3 (a) | 564.9 |
(a) Provided from our previous study [39].
