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. 2019 Sep 25;24(19):3480. doi: 10.3390/molecules24193480

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© 2019 by the authors.

Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).

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Syntheses of hexadentate mono-substituted triazine based linkers 6 and 7: a) in dioxane/water (10:1): Pd(dppf)Cl₂, KOAc (6a, 88%), Pd(PPh₃)₄, K₃PO₄ (6b, 83%; 6c, 81%). b) LiOH, H₂O (7a, quant.; 7b, quant.; 7c, 89%).