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Synthesis of a model di-behenoyl tri-arabinoglycerol (11, R = H). Reagents and conditions: (i) methanesulfonyl chloride (MsCl), 4-dimethylaminopyridine (DMAP), pyridine, 87%; (ii) CsHCO3, behenic acid, DMF/THF, 70 °C, (11, R = Bn, 80%); (iii) Pd(OH)2/C (20%), H2, 82%.
