Figure - PMC

Skip to main content

An official website of the United States government

Here's how you know

Here's how you know

Official websites use .gov
A .gov website belongs to an official government organization in the United States.

Secure .gov websites use HTTPS
A lock ( ) or https:// means you've safely connected to the .gov website. Share sensitive information only on official, secure websites.

View full-text article in PMC

. 2019 Oct 6;24(19):3596. doi: 10.3390/molecules24193596

Search in PMC
Search in PubMed
View in NLM Catalog
Add to search

© 2019 by the authors.

Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).

PMC Copyright notice

Scheme 5 — Synthesis of dimycoloyl triarabinoglycerol (DMTAG) glycolipids. (i) RCOOH (R’ = TBDMS) (12a–c), 1-ethyl-3-(3-dimethylaminopropyl)carbodi-imide (EDCI), DMAP, CH₂Cl₂ (a: 51%; b: 84%; c: 46%); (ii) TBAF, THF (a 76%; b: 51%; c: 66%); (iii) Pd(OH)₂/C (20%), H₂, CH₃OH:CH₂Cl₂: THF (1:1:1.5), rt, 36 h, (a: 86%; b: 88%; c: 82%).