Table 4.
Recovery of six BAs.
Extraction Samples | QC Samples | ||||||||
---|---|---|---|---|---|---|---|---|---|
Compounds | Original Amounts (g) | Spiked Amounts (mg) | Detected Amounts (mg) | Recovery (%) | Mean Recovery (%) | RSD (%) | QC Levels | Mean Recovery (%) | RSD (%) |
KBA | 0.04918 | 0.750 | 1.521 | 102.60 | 98.44 | 4.78 | L | 104.75 | 1.93 |
0.04726 | 0.750 | 1.423 | 93.45 | ||||||
0.05012 | 0.750 | 1.556 | 105.36 | M | 101.63 | 2.21 | |||
0.05035 | 0.750 | 1.498 | 97.15 | ||||||
0.04509 | 0.750 | 1.395 | 94.14 | H | 104.38 | 1.05 | |||
0.04728 | 0.750 | 1.457 | 97.94 | ||||||
AKBA | 0.04918 | 1.235 | 2.511 | 105.76 | 101.01 | 4.26 | L | 97.67 | 3.76 |
0.04726 | 1.235 | 1.376 | 98.63 | ||||||
0.05012 | 1.235 | 2.492 | 102.35 | M | 103.40 | 4.09 | |||
0.05035 | 1.235 | 2.390 | 93.64 | ||||||
0.04509 | 1.235 | 2.385 | 103.67 | H | 96.71 | 1.98 | |||
0.04728 | 1.235 | 2.418 | 102.00 | ||||||
α-BA | 0.04918 | 0.920 | 1.807 | 97.95 | 99.12 | 1.73 | L | 101.24 | 2.64 |
0.04726 | 0.920 | 1.772 | 97.99 | ||||||
0.05012 | 0.920 | 1.841 | 99.76 | M | 91.68 | 3.01 | |||
0.05035 | 0.920 | 1.820 | 97.02 | ||||||
0.04509 | 0.920 | 1.762 | 101.24 | H | 105.11 | 2.47 | |||
0.04728 | 0.920 | 1.798 | 100.77 | ||||||
β-BA | 0.04918 | 2.40 | 4.729 | 99.44 | 97.97 | 3.13 | L | 102.90 | 4.48 |
0.04726 | 2.40 | 4.598 | 97.79 | ||||||
0.05012 | 2.40 | 4.869 | 103.41 | M | 99.53 | 1.55 | |||
0.05035 | 2.40 | 4.704 | 96.08 | ||||||
0.04509 | 2.40 | 4.436 | 95.35 | H | 106.39 | 2.20 | |||
0.04728 | 2.40 | 4.550 | 102.60 | ||||||
α-ABA | 0.04918 | 0.318 | 0.607 | 92.54 | 97.88 | 4.86 | L | 102.35 | 3.14 |
0.04726 | 0.318 | 0.635 | 105.18 | ||||||
0.05012 | 0.318 | 0.641 | 101.35 | M | 98.17 | 1.58 | |||
0.05035 | 0.318 | 0.621 | 94.60 | ||||||
0.04509 | 0.318 | 0.589 | 95.05 | H | 101.04 | 4.22 | |||
0.04728 | 0.318 | 0.614 | 98.54 | ||||||
β-ABA | 0.04918 | 2.10 | 4.080 | 95.62 | 96.71 | 3.72 | L | 103.82 | 3.23 |
0.04726 | 2.10 | 3.891 | 90.47 | ||||||
0.05012 | 2.10 | 4.135 | 96.35 | M | 106.44 | 1.79 | |||
0.05035 | 2.10 | 4.202 | 99.08 | ||||||
0.04509 | 2.10 | 3.956 | 97.92 | H | 100.01 | 2.80 | |||
0.04728 | 2.10 | 4.11 | 100.86 |
L: LQC levels, M: MQC levels, H: HQC levels.