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. 2019 Oct 23;8(10):1303–1308. doi: 10.1002/open.201900222

Figure 1.

Figure 1

Synthesis of computer‐generated designs 1 and 2. Reagents & conditions: a) MsCl, NaN3, 4‐DMAP, CH2Cl2, DMF, −4 °C→rt, 4 h, 82 %; b) PPh3, H2O, THF, rt, 16 h, 90 %; c) 2‐phenylacetyl chloride (6), 4‐DMAP, THF, 0 °C→rt, 60 min., 92 %. d) neat, μw 80 °C, 1 h, 75 %.