Table 3.
Analyte (mg/l) | Components of measurement error | Mean of five runs | Sign statistic | P a |
---|---|---|---|---|
κFLC | Carryover | 1.2% | 5 | 0.0625 |
Drift | −0.018 | 2 | 1.0000 | |
λFLC | Carryover | 0.0% | 2 | 1.0000 |
Drift | −0.230 | 1 | 0.3750 |
The sign test was statistically significant at 6.25% significance level.