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. Author manuscript; available in PMC: 2019 Oct 25.
Published in final edited form as: J Am Chem Soc. 2019 Sep 16;141(38):15441–15449. doi: 10.1021/jacs.9b08504

Table 2.

Tandem SNAr-Ligand-Coupling Reactions To Form Nonsymmetrical Bis-Azine Biarylsa

graphic file with name nihms-1054592-t0002.jpg
a

Isolated yields are reported.

b

3f was formed using a two-stage protocol: 1.2 equiv of chloroazine, 2.2 equiv of NaOTf, TFE, 80 °C then 1.2 of equiv HCl and 10 equiv of water were added.

c

TfOH used instead of HCl.