Table 2.
Carbon No. | 1H NMR (δppm) | 13C NMR (δppm) |
---|---|---|
1 | - | 37.6 |
2 | - | 32.0 |
3 | 3.52 | 72.2 (CH) |
4 | - | 42.7 |
5 | - | 141.1 |
6 | 5.36 (H, dd) | 122.1 (CH) |
7 | - | 32.0 |
8 | - | 32.3 |
9 | - | 50.5 |
10 | - | 36.5 |
11 | - | 21.4 |
12 | - | 37.6 |
13 | - | 42.7 |
14 | - | 57.1 |
15 | - | 24.7 |
16 | - | 29.5 |
17 | - | 56.4 |
18 | 0.71 | 12.3 (CH) |
19 | 0.93 | 19.4 |
20 | - | 40.1 |
21 | 1.02 (H, d) | 21.4 (CH) |
22 | 5.36 | 138.7 (CH) |
23 | - | 129.6 |
24 | - | 50.5 |
25 | - | 32.0 |
26 | 0.82 (2H, d) | 19.1 (CH3) |
27 | 0.80 (2H, d) | 21.4 (CH3) |
28 | - | 24.7 (CH3) |
29 | 0.82 (2H, d) | 12.2 (CH3) |
H = hydrogen; C = Carbon; δppm = chemical shift; br = broad signal; s = singlet; d = doublet; dd=doublet of doublets; J = coupling constant; Hz = hertz; NMR = nuclear magnetic rasonance; CD3OD = Deuterated methanol.