Table 2.
ANOVA results for remaining activity and physical properties of microencapsulated TG
| Variation source | Remaining activity (%) | Moisture (%) |
L | a | b | ρp (kg/m3) |
ρb (kg/m3) |
ρt (kg/m3) |
CI (%) |
HR | ε (%) |
|---|---|---|---|---|---|---|---|---|---|---|---|
| p value | |||||||||||
| Model | < 0.0001 | < 0.0001 | 0.0129 | 0.0014 | 0.0011 | 0.0529 | 0.0006 | 0.0025 | 0.8417 | 0.4420 | < 0.0001 |
| Linear mixture | 0.0069 | < 0.0001 | 0.0009 | 0.0019 | 0.0020 | 0.1376 | < 0.0001 | < 0.0001 | 0.9778 | 0.9540 | < 0.0001 |
| X1 | 0.0115 | – | 0.6903 | 0.2753 | 0.4480 | 0.0726 | – | 0.0413 | – | – | – |
| X2 | 0.0244 | – | 0.8347 | 0.4169 | 0.2012 | 0.1527 | – | 0.5549 | – | – | – |
| C1C2 | 0.0023 | 0.6933 | – | 0.0020 | 0.0021 | 0.9936 | <0.0001 | < 0.0001 | – | 0.4563 | < 0.0001 |
| C1C3 | 0.0190 | 0.1210 | – | 0.1140 | 0.1301 | 0.0104 | 0.0016 | 0.0215 | – | 0.1622 | 0.1442 |
| C1X1 | < 0.0001 | – | 0.6128 | – | – | 0.9924 | 0.0752 | 0.9897 | 0.8807 | 0.9877 | – |
| C1X2 | < 0.0001 | – | 0.9677 | – | – | 0.4291 | 0.7613 | 0.3264 | 0.4099 | 0.3368 | – |
| C2C3 | 0.3258 | 0.0009 | – | 0.1521 | 0.1137 | 0.2211 | 0.7399 | 0.8861 | – | 0.8210 | 0.8002 |
| C2X1 | < 0.0001 | – | 0.4338 | – | – | 0.0250 | 0.9526 | 0.0591 | 0.8047 | 0.6052 | – |
| C2X2 | 0.0004 | – | 0.5562 | – | – | 0.5577 | 0.8537 | 0.3623 | 0.1705 | 0.4187 | – |
| C3X1 | 0.0009 | – | – | – | – | – | 0.0868 | – | 0.9437 | 0.7725 | – |
| C3X2 | 0.0118 | – | – | – | – | – | 0.1025 | – | 0.4520 | 0.4602 | – |
| C1C2C3 | 0.0061 | 0.0005 | – | – | – | 0.0991 | 0.5146 | 0.6353 | – | 0.9021 | – |
| C1C2X1 | 0.0541 | – | – | – | – | 0.3482 | 0.8567 | 0.0947 | – | 0.0197 | – |
| C1C2X2 | 0.1827 | – | – | – | – | 0.0454 | 0.9294 | 0.8323 | – | 0.4168 | – |
| C1C3X1 | 0.1146 | – | – | – | – | 0.6720 | 0.0481 | 0.0269 | – | 0.2981 | – |
| C1C3X2 | 0.5015 | – | – | – | – | 0.8771 | 0.7108 | 0.9489 | – | 0.2456 | – |
| C1X1X2 | 0.4258 | – | 0.0227 | – | – | 0.0466 | 0.1540 | 0.3902 | – | 0.5596 | – |
| C2C3X1 | 0.9463 | – | – | – | – | 0.9162 | 0.7041 | 0.9596 | – | 0.4626 | – |
| C2C3X2 | 0.7278 | – | – | – | – | 0.3003 | 0.4410 | 0.1022 | – | 0.0524 | – |
| C2X1X2 | 0.4095 | – | 0.7340 | – | – | 0.1756 | 0.2865 | 0.2570 | – | 0.7582 | – |
| C3X1X2 | 0.0217 | – | 0.8272 | – | – | 0.5534 | 0.9227 | 0.9807 | – | 0.5446 | – |
| C1X21 | 0.0834 | – | 0.1087 | – | – | – | 0.0119 | 0.0146 | – | 0.5117 | – |
| C2X21 | 0.0456 | – | 0.0285 | – | – | – | 0.5400 | 0.7507 | – | 0.6032 | – |
| C3X21 | 0.0034 | – | 0.1032 | – | – | – | 0.0833 | 0.0689 | – | 0.1639 | – |
| C1C2C3X1 | 0.1750 | – | – | – | – | 0.7798 | 0.1113 | 0.1753 | – | 0.9527 | – |
| C1C2C3X2 | 0.8267 | – | – | – | – | 0.0155 | 0.1057 | 0.3174 | – | 0.6709 | – |
| C1C2X1X2 | 0.3445 | – | – | – | – | 0.2031 | 0.0035 | 0.0852 | – | 0.2317 | – |
| C1C3X1X2 | 0.5542 | – | – | – | – | 0.7529 | 0.3749 | 0.3325 | – | 0.9576 | – |
| C2C3X1X2 | 0.0290 | – | – | – | – | 0.0326 | 0.2997 | 0.0729 | – | 0.0972 | – |
| C1C2X21 | 0.0011 | – | – | – | – | – | 0.2059 | 0.2059 | – | 0.6895 | – |
| C1C3X21 | 0.1888 | – | – | – | – | – | 0.7556 | 0.7575 | – | 0.2036 | – |
| C2C3X21 | 0.2574 | – | – | – | – | – | 0.3640 | 0.1683 | – | 0.1751 | – |
| C1C2C3X1X2 | 0.0078 | – | – | – | – | 0.6251 | 0.0105 | 0.0132 | – | 0.6251 | – |
| C1C2C3X21 | 0.0172 | – | – | – | – | – | 0.0598 | 0.0906 | – | 0.6078 | – |
| Lack of fit | 0.1635 | 0.8755 | 0.6267 | 0.7874 | 0.7155 | 0.6089 | 0.7694 | 0.6051 | 0.5317 | 0.7809 | 0.2817 |
| R2 | 0.9831 | 0.7343 | 0.5487 | 0.3807 | 0.3876 | 0.8334 | 0.9752 | 0.9655 | 0.1180 | 0.8451 | 0.6458 |
| Adj-R2 | 0.9020 | 0.7037 | 0.3111 | 0.2816 | 0.2896 | 0.4315 | 0.8559 | 0.8001 | − 0.0884 | 0.1016 | 0.6124 |
| C.V.% | 1.70 | 7.33 | 4.34 | 40.83 | 23.18 | 3.41 | 13.27 | 15.41 | 15.99 | 9.32 | 4.76 |
| Adeq. precision | 13.04 | 11.06 | 8.77 | 6.65 | 6.84 | 6.98 | 12.78 | 10.65 | 3.10 | 4.99 | 12.63 |
X1 homogenization time (min), X2 homogenization rate (rpm), C1 mannitol (%), C2 gum arabic (%), C3 casein (%)