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. 2019 Oct 3;75(Pt 11):1613–1619. doi: 10.1107/S2056989019013458

Table 4. Torsion angles τ 7, τ 8, τ 9, τ 10 and τ 11 (°) in related hydrazinecarbodi­thio­ates.

Two sets of torsion angles are stated for compounds EXINAB, QORJAK, SIMMUX, VOJGUX and WUPGIX because there are two mol­ecules in their asymmetric units. The mol­ecule with disorder in the structure of compound ZENLIN was omitted from this table.

Compound R1 τ 7 τ 8 τ 9 τ 10 τ 11
ABOROA (Manan et al., 2011) 5-fluoro-2-oxo-1,2-di­hydro-3H-indol-3-yliden­yl 175.1 5.0 −176.8 168.2 −98.3
ABORUG (Manan et al., 2011) 5-bromo-2-oxo-1,2-di­hydro-3H-indol-3-yliden­yl −178.5 −9.1 176.9 −108.0 −84.1
ABOSAN (Manan et al., 2011) 5-chloro-2-oxo-1,2-di­hydro-3H-indol-3-yliden­yl −178.8 −7.7 177.5 −110.4 −81.8
BAHWIT (Md Yusof et al., 2015) 2-meth­oxy­benzyl­iden­yl −179.1 2.6 −178.0 −177.7 −85.7
BAHWOZ (Md Yusof et al., 2015) 3-meth­oxy­benzyl­iden­yl −178.0 −1.2 −178.1 173.8 −80.1
CEFBIB (Islam et al., 2016a ) 2,4,5-tri­meth­oxy­benzyl­iden­yl 179.6 −5.2 −177.9 173.4 −79.7
COBQUH (Mirza et al., 2014) pyridin-2-yl­methylen­yl −177.2 −5.3 −177.2 −176.0 −68.7
DATFEK (Khoo et al., 2005) furan-2-yl)ethyl­iden­yl 178.6 1.7 180.0 180.0 −72.5
EDETUD (How et al., 2007) 1-(3-pyrid­yl)ethyl­iden­yl −179.2 4.9 −179.8 −165.8 −87.5
EHIXUQ (Yusof et al., 2016) 2-hy­droxy-3-meth­oxy­benzyl­iden­yl 177.4 1.8 179.9 −173.3 −101.2
EMEBAA (Ravoof et al., 2011) bis­(pyridin-2-yl)methylen­yl −165.7 1.4 175.4 176.2 −83.4
EPOFAR (Ali et al., 2011) 2-oxo-1,2-di­hydro-3H-indol-3-yliden­yl 176.5 −4.5 −176.2 165.0 −95.5
EVITUZ (Shan et al., 2011a ) 2-nitro­benzyl­iden­yl 170.6 3.6 179.4 −80.1 132.1
EXINAB (Shan et al., 2011b ) 2-methyl­benzyl­iden­yl −174.0 −176.9 −2.7 −4.9 −178.7 −177.4 174.2 175.6 −68.2 −68.7
GUMJUV (Break et al., 2013) 4-chloro­phen­yl)ethyl­iden­yl −172.7 −0.3 −179.3 86.8 68.1
HELZIK (Omar et al., 2018) 1-(6-methyl­pyridin-2-yl)ethyl­iden­yl −177.7 −1.6 −176.0 171.6 −108.0
IFUTUZ (Khaledi et al., 2008a ) 1H-indol-3-yl­methyl­iden­yl −172.7 2.6 179.0 103.7 −68.2
JAMMOA (Ali et al., 2004) quinolinyl-2-methylen­yl 177.9 0.8 177.5 −171.0 101.8
KAGZOK (Ravoof et al., 2015) 1-(5-methyl­pyridin-2-yl)ethyl­iden­yl −176.9 −5.6 −173.2 164.7 −77.8
KUCRAC (Hamid et al., 2009) 1-(pyrazin-2-yl)ethyl­iden­yl 178.4 0.6 178.8 174.7 −70.0
KUCZUD (Xu et al., 1991) pyridine-N-oxide-2-yl)methyl­iden­yl −171.4 −2.0 176.5 −161.7 −92.2
LOBSEB (Shan et al., 2008b ) furan-2-yl­methylen­yl 173.8 −0.5 179.7 177.1 −93.0
LOBVOO (Tarafder et al., 2008) (E)-3-phenyl­allyl­iden­yl −177.4 3.0 177.6 −175.3 −102.7
LOJBUI (Khaledi et al., 2008b ) 1-methyl-1H-indol-2-yl­methylen­yl 179.1 −2.3 −179.1 172.9 −78.9
LOJLIG (Khaledi et al., 2008b ) di­phenyl­methylen­yl 170.5 −1.2 −175.2 164.8 −83.8
LUBNIH (Zangrando et al., 2015) 1-(3-hy­droxy­phen­yl)ethyl­iden­yl −177.5 −0.8 173.7 180.0 −71.1
NIZBUV (Omar et al., 2014) 1-(4-methyl­pyridin-2-yl)ethyl­iden­yl −178.4 0.0 −175.8 −95.9 −141.1
OQOWOH (Akbar Ali et al., 2011) bis­(pyridin-2-yl)methylen­yl 165.1 1.9 −177.2 −180.0 −83.8
PEWLEL (Li et al., 2012) phen­yl(pyridin-2-yl)methylen­yl −177.0 4.6 −173.1 87.6 −119.2
QORJAK (Tan et al., 2015) 3,4-di­meth­oxy­benzyl­iden­yl 169.2 −170.4 −3.1 3.7 −179.5 175.1 169.5 −168.8 −118.8 −105.7
QUCLIL (Biswal et al., 2015) 1-(2-hy­droxy­phen­yl)ethyl­idene2-hy­droxy­phen­yl)ethyl­iden­yl 176.7 0.6 −173.3 171.2 −115.5
RIYZOP (Shan et al., 2008a ) benzyl­iden­yl 177.1 0.1 178.5 171.8 −80.0
RUGLAH (Li et al., 2009) 3-nitro­benzyl­iden­yl 178.3 −2.9 −177.5 173.1 −85.5
SALSEE (Zhang et al., 2004) 4-((2-hy­droxy­eth­yl)methyl­amino)­benzyl­iden­yl −166.4 0.9 −176.8 170.4 −88.4
SIMMUX (Qiu & Luo, 2007) 2-bromo­benzyl­iden­yl 175.6 −173.9 2.6 −5.6 178.8 −176.3 −170.6 173.6 −115.6 75.2
TADVEC (Islam et al., 2016b ) 3,4,5-tri­meth­oxy­benzyl­iden­yl −179.4 −5.1 −177.1 174.9 −73.3
TIFSEH (Roy et al., 2007) 2-methyl­thio-6-methyl-4-pyrimid­yl)methylen­yl −177.8 0.6 −178.4 164.9 −76.6
UWATOD (Flörke & Boshaala, 2016) 1-phenyl­ethyl­iden­yl 172.4 −4.0 −173.3 159.5 −102.0
VOJCUT (Khaledi et al., 2008c ) 1-methyl-1H-indol-3-yl­methyl­iden­yl −177.2 −1.7 −176.0 −101.3 −129.4
VOJGUX (Shi et al., 2008) 2-chloro­benzyl­iden­yl −174.7 178.3 −2.0 0.3 −179.3 176.9 −174.0 −174.1 −80.3 −110.1
WADGAK (Chan et al., 2003) 1-(thio­phen-2-yl)ethyl­iden­yl 174.8 −5.8 177.8 77.6 17.1
WUPGIX (Tarafder et al., 2002) 5-methyl­furan-2-yl)methylen­yl −169.2 179.8 −0.2 1.5 179.7 −176.3 −173.6 −171.7 −100.8 −77.9
YAHDAO (Fan et al., 2011a ) 4-meth­oxy­benzyl­iden­yl −175.8 1.4 −179.5 −178.9 −87.9
YAHDUI (Fan et al., 2011b ) 2-bromo-5-meth­oxy­benzyl­iden­yl 177.8 −3.6 −176.0 174.9 119.2
ZENLIN (Fun et al., 1995) 4-(di­methyl­amino)­benzyl­iden­yl −180.0 1.3 179.9 −178.0 −97.1