Table 5. Experimental details.
| Crystal data | |
| Chemical formula | C22H15Cl2NOS |
| M r | 412.31 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 150 |
| a, b, c (Å) | 9.0373 (7), 16.6798 (13), 12.511 (1) |
| β (°) | 95.982 (2) |
| V (Å3) | 1875.6 (3) |
| Z | 4 |
| Radiation type | Cu Kα |
| μ (mm−1) | 4.25 |
| Crystal size (mm) | 0.15 × 0.13 × 0.09 |
| Data collection | |
| Diffractometer | Bruker D8 VENTURE PHOTON 100 CMOS |
| Absorption correction | Numerical (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.59, 0.70 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 48886, 3847, 3650 |
| R int | 0.038 |
| (sin θ/λ)max (Å−1) | 0.625 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.026, 0.070, 1.05 |
| No. of reflections | 3847 |
| No. of parameters | 304 |
| H-atom treatment | All H-atom parameters refined |
| Δρmax, Δρmin (e Å−3) | 0.22, −0.26 |