Table 5.
№ | 14g | 14h | 14i | 14j | 14k |
---|---|---|---|---|---|
H-2 | s 7.91 | s 7.99 | s 8.00 | s 8.00 | s 7.89 |
H-5 | d 7.00 (J = 9.3 Hz) |
m 7.04 | m 7.02 | d 7.05 (J = 8.5 Hz) | d 7.03 (J = 8.5 Hz) |
H-6 | m 7.62 | m 7.72 | m 7.69 | bs 7.75 | m 7.63 |
H-7 | s 3.80 | s 3.85 | s 3.83 | s 3.83 | s 3.81 |
H-8 | s 8.14 | s 8.14 | s 8.11 | s 8.15 | s 7.97 |
H-9 | s 4.09 | s 5.00 | s 3.55 | s 3.68 | s 5.21 |
H-10 | bs 2.57 | bs 2.69 | |||
H-11 | s 1.19 (t-Bu) | bs 3.07 | bs 2.93 | ||
H-12 | s 7.09 | s 2.28 (Me) | |||
H-13 | s 7.18 | m 7.06 | m 6.90 | m 6.87–6.94 | 2.34 |
H-14 | s 2.21 (Me) | m 7.28 | m 7.02 | m 6.87–6.94 | 2.67 |
H-15 | s 7.09 | m 6.86 | m 6.87–6.94 | ||
H-16 | m 7.02 | m 6.87–6.94 | |||
H-17 | m 6.90 | s 3.74 (OMe) | |||
NH | s 11.32 | s 11.33 | s 11.29 | s 11.34 | s 11.33 |
NH2 | s 7.62 and s 7.80 | s 7.89 and s 7.93 |
m 7.69 and s 7.85 | bs 7.72 and bs 7.90 | s 7.75 and s 7.78 |