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. 2019 Oct 15;24(20):3711. doi: 10.3390/molecules24203711

Table 5.

NMR 1H spectra of 14f–14k (DMSO-d6, δ).

graphic file with name molecules-24-03711-i031.jpg

14g 14h 14i 14j 14k
H-2 s 7.91 s 7.99 s 8.00 s 8.00 s 7.89
H-5 d 7.00
(J = 9.3 Hz)
m 7.04 m 7.02 d 7.05 (J = 8.5 Hz) d 7.03
(J = 8.5 Hz)
H-6 m 7.62 m 7.72 m 7.69 bs 7.75 m 7.63
H-7 s 3.80 s 3.85 s 3.83 s 3.83 s 3.81
H-8 s 8.14 s 8.14 s 8.11 s 8.15 s 7.97
H-9 s 4.09 s 5.00 s 3.55 s 3.68 s 5.21
H-10 bs 2.57 bs 2.69
H-11 s 1.19 (t-Bu) bs 3.07 bs 2.93
H-12 s 7.09 s 2.28 (Me)
H-13 s 7.18 m 7.06 m 6.90 m 6.87–6.94 2.34
H-14 s 2.21 (Me) m 7.28 m 7.02 m 6.87–6.94 2.67
H-15 s 7.09 m 6.86 m 6.87–6.94
H-16 m 7.02 m 6.87–6.94
H-17 m 6.90 s 3.74 (OMe)
NH s 11.32 s 11.33 s 11.29 s 11.34 s 11.33
NH2 s 7.62 and s 7.80 s 7.89 and
s 7.93
m 7.69 and s 7.85 bs 7.72 and bs 7.90 s 7.75 and
s 7.78