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. 2019 Oct 15;24(20):3711. doi: 10.3390/molecules24203711

Table 13.

NMR1H spectra of 16p16r (CDCl3 for 16o and DMSO-d6 for 16p,q; δ).

16p 16q 16r
Structure graphic file with name molecules-24-03711-i063.jpg graphic file with name molecules-24-03711-i064.jpg graphic file with name molecules-24-03711-i065.jpg
H-14 s 7.24 s 7.22 s 7.12
H-17 s 8.30 s 8.33 s 7.68
H-19 m 8.21 d 6.69 (J = 3.3 Hz,
AB-system)
H-20 d 6.66 (J = 3.3 Hz,
AB-system)
H-21 s 7.45 m 7.34
H-22 m 7.21 m 7.13
H-23 m 7.21 m 7.13 s 7.62
H-24 d 7.83 (J = 2.7 Hz) m 8.10
H-25 d 7.52 (J = 7.5 Hz)
H-26 s 2.51 m 7.21–7.30
H-27 m 7.21–7.30
NH s 12.08 s 12.00 ---
NH (HetAr) s 11.59 s 11.51
OH-3 bs 18.82 bs 18.82 s 18.76
OH-7 s 13.03 bs 13.05 ---
OH-9 s 10.30 s 10.31 s 10.26