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. 2019 Oct 15;24(20):3711. doi: 10.3390/molecules24203711

Table 16.

NMR 13C spectra of 17a17f (CDCl3, δ).

17a 17b 17c 17d 17e 17f
C-17 142.43 143.82 143.09 142.48 142.30 142.35
C-18 125.64 125.43 125.30 125.01 124.84 125.12
C-19 127.14 127.14 127.13 127.07 127.11 127.14
C-20 126.07 125.93 126.00 126.04 126.20 126.28
C-21 158.06 158.19 158.08 158.03 158.10 158.05
C-22 110.26 110.21 110.14 110.25 110.41 110.34
C-23 127.69 128.96 127.93 127.96 128.06 128.65
C-24 65.26 65.91 65.88 65.32 65.16 65.22
C-25 55.47 55.46 55.36 55.46 55.53 55.78
C-26 d 154.74
(J = 2.2 Hz)
d 146.61 (J = 10 Hz) d 146.61 (J = 11 Hz) d 154.81 (J = 2.4 Hz) t 160.57 (J = 13.4 Hz) d 150.14 (J = 2.4 Hz)
C-27 d 115.56
(J = 12 Hz)
115.50 d 151.42 (J = 247 Hz) 116.44 d 162.68 (J = 244 Hz) d 121.50 (J = 10 Hz)
C-28 d 115.83
(J = 3.2 Hz)
d 151.84
(J = 249 Hz)
d 116 (J = 16 Hz) 120.83 (J = 19 Hz) t 96.47 (J = 29 Hz) d 118.51 (J = 28 Hz)
C-29 d 155.68
(J = 239 Hz)
d 116.00
(J = 19 Hz)
d 121.24 (J = 7 Hz) d 151.54 (J = 247 Hz) d 162.55 (J = 244 Hz) d 156.08 (J = 247 Hz)
C-30 d 115.83
(J = 3.2 Hz)
d 124.08
(J = 3.5 Hz)
d 124.10 (J = 3.4 Hz) d 116.51 (J = 22 Hz) m 98.50 d 114.06 (J = 21 Hz)
C-31 d 115.56
(J = 12 Hz)
d 121.25
(J = 8 Hz)
115.41 d 114.30 (J = 6.7 Hz) m 98.50 d 114.67 (J = 9.4 Hz)