Table 2.
Calibration curve, linearity, LOD, LOQ, and %SSE of the optimized method.
Mycotoxin | Calibration Curve | R 2 | LOD (μg/kg) | LOQ (μg/kg) | SSE (%) | ||
---|---|---|---|---|---|---|---|
Calibration Range (μg/kg) | Slope | Intercept | |||||
AFB1 | 0.5−20 | 10,644.3 | −142.4 | 0.9999 | 0.08 | 0.26 | 89.7 |
AFB2 | 0.5−20 | 8025.6 | −834.4 | 0.9998 | 0.14 | 0.43 | 94.6 |
AFG1 | 0.5−20 | 8873.9 | 394.8 | 0.9999 | 0.10 | 0.30 | 100.8 |
AFG2 | 0.5−20 | 6878.5 | −722.1 | 0.9999 | 0.15 | 0.45 | 98.7 |
OTA | 0.5−20 | 20,887.2 | 8984.6 | 0.9998 | 0.06 | 0.17 | 87.0 |
ZEN | 25−1000 | 4638.2 | −5420.4 | 0.9999 | 4.68 | 14.18 | 96.7 |
ZAN | 25−1000 | 11,972.7 | −8964.7 | 1.0000 | 1.66 | 5.03 | 95.5 |
α-ZEL | 25−1000 | 700.0 | −716.6 | 0.9999 | 1.47 | 4.44 | 94.2 |
α-ZAL | 25−1000 | 2098.0 | 2773.7 | 0.9998 | 2.29 | 6.94 | 95.9 |
β-ZEL | 25−1000 | 3649.0 | −12,582.2 | 1.0000 | 1.72 | 5.23 | 99.5 |
β-ZAL | 25−1000 | 2042.0 | 8338.2 | 0.9997 | 2.13 | 6.45 | 101.9 |
T-2 | 25−1000 | 23,047.8 | 411,783.3 | 0.9995 | 2.55 | 7.73 | 103.8 |
HT-2 | 25−1000 | 18,293.4 | 257,935.3 | 0.9994 | 1.86 | 5.65 | 93.1 |
NIV | 25−1000 | 1423.3 | −6891.8 | 0.9999 | 3.21 | 9.74 | 98.2 |
DON | 25−1000 | 941.3 | −3171.0 | 1.0000 | 4.37 | 13.24 | 98.0 |
3ADON | 25−1000 | 821.9 | −5844.9 | 0.9999 | 0.9 | 2.73 | 100.4 |
D3G | 25−1000 | 6246.2 | −12,849.3 | 0.9999 | 2.72 | 8.24 | 100.3 |
FB1 | 25−1000 | 22,786.0 | −127,037.2 | 0.9998 | 2.57 | 7.78 | 98.1 |
FB2 | 25−1000 | 24,992.8 | −211,390.0 | 1.0000 | 2.16 | 6.56 | 87.1 |
FB3 | 25−1000 | 19,609.8 | −21,763.0 | 1.0000 | 2.22 | 6.72 | 86.5 |