Table 4.
Mycotoxin | Spiking Level (μg/kg) | Expanded Uncertainty | Uncertainty/Result (%) | Mycotoxin | Spiking Level (μg/kg) | Expanded Uncertainty | Uncertainty/Result (%) |
---|---|---|---|---|---|---|---|
AFB1 | 1 | 0.23 | 22.7 | β-ZAL | 15 | 1.18 | 15.8 |
2 | 0.31 | 15.4 | 37 | 3.28 | 17.7 | ||
3 | 0.73 | 14.6 | 74 | 7.53 | 20.3 | ||
6 | 1.26 | 12.6 | 148 | 12.93 | 17.5 | ||
AFB2 | 1 | 0.20 | 19.8 | T-2 | 15 | 2.38 | 31.7 |
2 | 0.31 | 15.3 | 37 | 2.40 | 13.0 | ||
3 | 0.69 | 13.8 | 74 | 2.92 | 7.9 | ||
6 | 1.32 | 13.2 | 148 | 6.02 | 8.1 | ||
AFG1 | 1 | 0.20 | 20.3 | HT-2 | 15 | 2.86 | 19.1 |
2 | 0.31 | 15.5 | 37 | 7.23 | 39.1 | ||
3 | 0.72 | 14.4 | 74 | 9.85 | 26.6 | ||
6 | 1.39 | 13.9 | 148 | 18.92 | 25.6 | ||
AFG2 | 1 | 0.20 | 19.6 | NIV | 15 | 1.10 | 14.7 |
2 | 0.32 | 15.8 | 37 | 1.76 | 9.5 | ||
3 | 0.72 | 14.3 | 74 | 4.33 | 11.7 | ||
6 | 1.35 | 13.5 | 148 | 11.86 | 16.0 | ||
OTA | 1 | 0.41 | 41.3 | DON | 15 | 0.69 | 9.2 |
2 | 0.83 | 41.6 | 37 | 1.89 | 10.2 | ||
3 | 1.42 | 28.4 | 74 | 3.88 | 10.5 | ||
6 | 3.11 | 31.1 | 148 | 10.49 | 14.2 | ||
ZEN | 15 | 2.02 | 13.4 | 3ADON | 15 | 0.85 | 11.4 |
37 | 7.21 | 19.5 | 37 | 2.18 | 11.8 | ||
74 | 16.66 | 22.5 | 74 | 4.30 | 11.6 | ||
148 | 29.22 | 19.7 | 148 | 10.16 | 13.7 | ||
ZAN | 15 | 1.95 | 13.0 | D3G | 15 | 0.78 | 10.3 |
37 | 8.56 | 23.1 | 37 | 1.50 | 8.1 | ||
74 | 22.02 | 29.8 | 74 | 3.09 | 8.3 | ||
148 | 47.40 | 32.0 | 148 | 11.45 | 15.5 | ||
α-ZEL | 15 | 2.01 | 13.4 | FB1 | 15 | 1.00 | 6.7 |
37 | 5.84 | 15.8 | 37 | 1.22 | 6.6 | ||
74 | 14.41 | 19.5 | 74 | 2.40 | 6.5 | ||
148 | 33.21 | 22.4 | 148 | 10.74 | 14.5 | ||
α-ZAL | 15 | 2.66 | 17.8 | FB2 | 15 | 0.50 | 6.7 |
37 | 7.80 | 21.1 | 37 | 2.86 | 15.4 | ||
74 | 14.86 | 20.1 | 74 | 4.80 | 13.0 | ||
148 | 25.70 | 17.4 | 148 | 17.58 | 23.8 | ||
β-ZEL | 15 | 2.25 | 15.0 | FB3 | 15 | 0.53 | 7.0 |
37 | 6.57 | 17.7 | 37 | 2.77 | 15.0 | ||
74 | 17.36 | 23.5 | 74 | 3.28 | 8.9 | ||
148 | 38.32 | 25.9 | 148 | 16.22 | 21.9 |