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. 2019 Jul 22;10(35):8202–8210. doi: 10.1039/c9sc02185j

Fig. 4. Monitoring the reaction progress between 1h and 2b by PXRD analysis. Conditions: 1h (0.3 mmol), 2b (0.36 mmol), Pd(OAc)2 (0.009 mmol), DavePhos (0.0135 mmol), CsF (0.9 mmol), H2O (20 μL), and 1,5-cod (0.12 μL mg–1) in a stainless-steel ball-milling jar (1.5 mL) with a stainless-steel ball (5 mm).

Fig. 4