Table 2. The analytical conditions for gas chromatography.
Parameters | Conditions |
---|---|
Instrument | ACME 6500 Gas chromatography (Young Lin Co., Korea) |
Detector | FID (Flame ionization detector) |
Column | HP-FFAP (25 m×0.32 mm×0.52 μm, Supelco, USA) |
Air & hydrogen flow rate | 350 & 35 (mL/min) |
Injector temperature | 230°C (splitless mode) |
Carrier gas | He |
Flow rate | 1.0 mL/min |
Detector temperature | 250°C (Temperature rising Mode) |
Oven temperature | Hold 3 min at 40°C
→ increase 10°C/min up to 120°C → increase 5°C/min up to 200°C |