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Summary of method validation parameters.
| Substance | LOD (ng g−1) |
LOQ (ng g−1) |
Average recovery (%) (n = 3) | Cross validation (CV %) recovery (n = 3) |
|---|---|---|---|---|
| Flupyradifurone | 19.72 | 65.73 | – | – |
| Thiacloprid | 7.61 | 25.36 | 64.3 | 6 (0.6 μg mL−1) |
1Concentrations at which CV was assessed are shown in brackets. Area values are listed in supplementary table S3.
