Table 1.
Citric Acid/EDTA Ratio | Size in Solution DLS (nm) | Polydispersity | Crystallite Size via XRD (nm) | Zeta Potential (mV) |
---|---|---|---|---|
100/0 | 7.8 | 0.374 | 2.0 | −20.8 |
70/30 | 3.8 | 0.309 | 2.3 | −20.4 |
60/40 | 2.6 | 0.198 | 2.4 | −18.7 |
50/50 | 2.7 | 0.188 | 2.4 | −21.5 |
40/60 | 2.9 | 0.162 | 2.5 | −18.3 |
30/70 | 3.0 | 0.188 | 2.5 | −23.0 |
20/80 | 3.5 | 0.160 | 2.4 | −9.1 |
0/100 | 2.4 | 0.230 | 2.1 | −15.70 |