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. Author manuscript; available in PMC: 2020 Aug 6.
Published in final edited form as: Biochemistry. 2019 Jul 26;58(31):3340–3353. doi: 10.1021/acs.biochem.9b00326

Table 4.

13C NMR Chemical Shifts (parts per million)

substrate C1 C2 C3 C4 C5
D-xyluluronatea 66.02 212.37 77.05 73.15 176.90
D-xyluluronateb 65.99 212.38 76.88 73.05 177.13
D-ribuluronateb 66.21 211.13 77.88 74.62 176.43
a

Produced from glyoxylate and DHAP with YdjI after dephosphorylation.

b

As reported previously.48