Table 3.
Validation runs with the values predicted by the model and the actual values measured by oxime titration. Predicted values were calculated from the optimized model in Equation (1).
|
Run |
A |
B |
C |
Aldehyde content [mmol g−1] |
|
|---|---|---|---|---|---|
|
|
[min] |
[h] |
[equiv.] |
Predicted |
Actual[b] |
|
1 |
2.0 |
7.9 |
1.625 |
6.3 |
6.9 |
|
2[c] |
2.4 |
5.0 |
1.625 |
4.5 |
4.2 |
|
3[c] |
2.0 |
8.0 |
1.25 |
6.9 |
8.0 |
|
4 |
2.0 |
8.0 |
2.00 |
5.8 |
5.0 |
|
5 |
2.0 |
1.0 |
2.00 |
1.4 |
0.9 |
|
6 |
11 |
4.5 |
1.25 |
4.0 |
4.0 |
|
7 |
20 |
8.0 |
2.00 |
2.3 |
2.5 |
[a] A=milling time; B=resting time; C=ratio of NaIO4/cellulose (molar equiv.)[b] Mean values from duplicate measurements. [c] Run 2 is denoted as DAC_34 % and run 3 as DAC_64 %.