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. 2019 Dec 2;9:18063. doi: 10.1038/s41598-019-54219-6

Figure 3.

Figure 3

DSC curves of the hydrothermal synthesis at 130 °C products after: 1–0 h, 2–4 h, 3–8 h, 4–12 h, 5–24 h, 6–36 h and 7–48 h.