Table 3.
Accuracy, intra- and interday precision of the standard compounds in DQ.
Compound | Spiked Amount (mg/mL) |
Content (mg/mL) | Recovery Test (%, n = 5) |
Precision Test (n = 5) | ||
---|---|---|---|---|---|---|
Un-Spiked | Measured | Intra-Day RSDa(%) |
Inter-Day RSD (%) |
|||
1 | 0.012 | 0.081910 | 0.0820287 | 101.0 | 0.24 | 0.55 |
0.04 | 0.109910 | 0.1073792 | 93.7 | 1.91 | 0.15 | |
0.12 | 0.189910 | 0.188932 | 99.2 | 0.62 | 0.28 | |
2 | 0.012 | 0.130902 | 0.1316462 | 106.2 | 0.31 | 0.73 |
0.04 | 0.158902 | 0.1582045 | 98.3 | 0.75 | 0.50 | |
0.12 | 0.238902 | 0.2368625 | 98.3 | 1.15 | 0.48 | |
4 | 0.012 | 0.212048 | 0.2116199 | 96.4 | 0.41 | 0.38 |
0.04 | 0.240048 | 0.2400817 | 100.1 | 0.44 | 0.75 | |
0.12 | 0.320048 | 0.3210118 | 100.8 | 0.26 | 0.52 | |
5 | 0.012 | 0.192213 | 0.1918098 | 96.6 | 0.27 | 0.29 |
0.04 | 0.220213 | 0.2220230 | 104.5 | 0.67 | 0.70 | |
0.12 | 0.300213 | 0.2928230 | 93.8 | 0.82 | 0.33 |
a RSD: relative standard deviation.