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. 2019 Nov 15;75(Pt 12):1866–1870. doi: 10.1107/S2056989019015159
Bruker APEXII area detector diffractometer 2453 independent reflections
Radiation source: fine-focus sealed tube 1798 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.045
φ and ω scans θmax = 28.3°, θmin = 1.5°
Absorption correction: for a sphere [the interpolation procedure of Dwiggins (1975) was used with some modification] h = −12→12
Tmin = 0.861, Tmax = 0.862 k = −10→10
15317 measured reflections l = −34→35