| Bruker APEXII area detector diffractometer | 2453 independent reflections |
| Radiation source: fine-focus sealed tube | 1798 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.045 |
| φ and ω scans | θmax = 28.3°, θmin = 1.5° |
| Absorption correction: for a sphere [the interpolation procedure of Dwiggins (1975) was used with some modification] | h = −12→12 |
| Tmin = 0.861, Tmax = 0.862 | k = −10→10 |
| 15317 measured reflections | l = −34→35 |