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. 2019 Nov 15;75(Pt 12):1871–1874. doi: 10.1107/S2056989019015238

Table 2. Experimental details.

Crystal data
Chemical formula [K2Pt(CN)4(C12H24O6)2]
M r 905.99
Crystal system, space group Monoclinic, P21/n
Temperature (K) 100
a, b, c (Å) 11.7341 (10), 13.7280 (12), 11.8876 (10)
β (°) 94.999 (3)
V3) 1907.6 (3)
Z 2
Radiation type Mo Kα
μ (mm−1) 3.96
Crystal size (mm) 0.44 × 0.44 × 0.12
 
Data collection
Diffractometer Bruker APEXII CCD
Absorption correction Multi-scan (SADABS; Bruker, 2016)
T min, T max 0.306, 0.564
No. of measured, independent and observed [I > 2σ(I)] reflections 57788, 5839, 4658
R int 0.047
(sin θ/λ)max−1) 0.716
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.019, 0.051, 1.05
No. of reflections 5839
No. of parameters 215
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 1.25, −1.54

Computer programs: APEX2 and SAINT (Bruker, 2016), SHELXS (Sheldrick, 2008), SHELXL2018 (Sheldrick, 2015), OLEX2 (Dolomanov et al., 2009) and publCIF (Westrip, 2010).