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. 2019 Oct 15;58(48):17273–17276. doi: 10.1002/anie.201911005

Figure 3.

Figure 3

Total volume versus time for burette method and bubble counter method. Reaction conditions: ammonia borane (0.40 mmol) in water (6.4 mL), 5 % Ru/C (2.0 mg) under stirring (1000 rpm) at 23 °C. The inset shows the final volume measured using burette and bubble counter with 95 % confidence intervals.