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1H and 13C NMR assignments for HD871-1 in CDCl3, referenced to internal TMS at 0.00 ppm
| Position | HD871-1 |
|
|---|---|---|
| δH/ppm, m (J/Hz) | δC/ppm | |
| 1 | 2.51, m; 2.27, ddt (18.0, 10.5, 2.5) | 31.5 |
| 2 | 6.73, m | 143.3 |
| 3 | 135.9 | |
| 4 | 198.4 | |
| 5 | 2.55, ddd (16.0, 3.9, 1.4); 2.44, dd (16.0, 12.8) | 42.8 |
| 6 | 3.35, m | 36.1 |
| 7 | 148.0 | |
| 8 | 194.5 | |
| 9 | 5.31, dd (9.2, 7.1) | 77.0 |
| 10 | 2.62, m; 2.02, m | 33.1 |
| 11 | 2.75, m | 34.7 |
| 12 | 178.2 | |
| 13 | 1.31, d (7.1) | 15.5 |
| 14 | 6.23, s; 6.00, s | 127.0 |
| 15 | 1.80, s | 16.1 |
