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. 2019 Dec 11;9:18806. doi: 10.1038/s41598-019-54933-1

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© The Author(s) 2019

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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This is a schematic representation of the chemical shifts for each of the seven fucosylated glycan and substrate α-L-fucose crosspeaks. The mean crosspeak volume for all thirty-three healthy volunteers. Fuc I, IV, III, IV, V and VI (in orange) all resonate at 1.36 ppm on the F1 axis but differ in F2. The Fuc II crosspeak (Yellow) is at 1.14 ppm in F1 and is reproducibly smaller than all the other crosspeaks. The α-L-fucose substrate crosspeaks are not present in 10 out of 33 of the healthy controls but are included in Fig. 4 as the mean average from the 23 times they were present.