Appendix 1—table 2. HPLC Purity of final compounds.
Compound | Retention time | Purity [%] | HPLC method* |
---|---|---|---|
1 | 3.27 min | 99 | B |
2 | 1.31 min | 99 | A |
3 | 1.52 min | 99 | A |
4 | 1.25 min | 99 | A |
5 | 1.18 min | 99 | A |
6 | 1.21 min | 99 | A |
7 | 1.17 min | 99 | A |
*Method A: in 2.2 min from 100% A to 100% D, then staying on 100% D. Method B: in 7.5 min from 100% A to 100% D, then staying on 100% D.