Table 3.
Potential intestinal lavage fluid biomarkers in the rat model of chronic migraine induced by nitroglycerin.
| NO | Retention Time | Name | Formula | Ion Mode | Error (ppm) | MS/MS |
|---|---|---|---|---|---|---|
| I1 | 11.03 | omega-Muricholate | C24H40O5 | [M-H]- | -0.12 | 389.2695, 289.2176, 209.1544, 195.1758 |
| I2 | 0.88 | Lysine | C6H14N2O2 | [M-H]- | 0.14 | 131.0826, 113.0732 |
| I3 | 0.81 | glutamic acid | C5H9NO4 | [M-H]- | -0.07 | 128.0355, 102.0546 |
| I4 | 0.74 | L-Arginine | C6H14N4O2 | [M-H]- | -0.12 | 131.0826, 156.0732, 68.9956 |
| I5 | 3.54 | 3-Indoxyl sulfate | C8H7NO4S | [M-H]- | -0.14 | 132.0454, 80.9655 |
| I6 | 11.03 | SM(d18:1/20:0) | C43H87N2O6P | [M+Br]- | -0.20 | 429.2628, 407.2809, 251.2020, 195.1758 |
| I7 | 3.59 | dihydroxyphenylalanine | C9H11NO4 | [M-H2O-H]- | 0.11 | 178.0507, 134.0613 |
| I8 | 3.04 | L-Tryptophan | C11H12N2O2 | [M+H]+ | -1.12 | 159.0952, 144.0831, 118.0683, 90.0482, 75.0249 |
| I9 | 2.65 | L-Phenylalanine | C9H11NO2 | [M+H]+ | 1.81 | 119.9480, 103.0005 |
| I10 | 2.22 | L-Tyrosine | C9H11NO3 | [M+H]+ | -0.77 | 135.8930, 95.0005 |
| I11 | 0.83 | L-Valine | C5H11NO2 | [M+H]+ | -0.85 | 118.0862, 78.0805 |
| I12 | 15.69 | 11-beta-hydroxyan- drosterone-3-glucuronide | C25H38O9 | [M+Na]+ | 2.47 | 289.2164, 177.0396 |