Table 1.
Yields shown are for pure isolated material. Products 8–13 were conducted on 0.5 mmol scale (15 mol% 2, 100 °C, 1 M toluene) and 14–19 were conducted on 1-gram scale (20 mol% 2, 120 °C, 1 M butyl acetate). 2 equiv of phenylsilane in all reactions.