Table 5. Experimental details.
| Crystal data | |
| Chemical formula | C24H21N5O·H2O |
| M r | 413.47 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 150 |
| a, b, c (Å) | 9.0872 (2), 21.1012 (4), 11.7134 (2) |
| β (°) | 112.654 (1) |
| V (Å3) | 2072.77 (7) |
| Z | 4 |
| Radiation type | Cu Kα |
| μ (mm−1) | 0.70 |
| Crystal size (mm) | 0.18 × 0.08 × 0.01 |
| Data collection | |
| Diffractometer | Bruker D8 VENTURE PHOTON 100 CMOS |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.85, 0.99 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 15080, 3887, 2909 |
| R int | 0.057 |
| (sin θ/λ)max (Å−1) | 0.610 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.048, 0.113, 1.06 |
| No. of reflections | 3887 |
| No. of parameters | 280 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.22, −0.22 |