Table 4. Experimental details.
| Crystal data | |
| Chemical formula | [Ag2(SCN)2(C2H3N3S)4] |
| M r | 736.44 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 100 |
| a, b, c (Å) | 4.8718 (1), 15.9511 (1), 13.9575 (1) |
| β (°) | 96.945 (1) |
| V (Å3) | 1076.69 (2) |
| Z | 2 |
| Radiation type | Cu Kα |
| μ (mm−1) | 20.35 |
| Crystal size (mm) | 0.41 × 0.14 × 0.11 |
| Data collection | |
| Diffractometer | Rigaku Oxford Diffraction SuperNova, Dual, Cu at zero, AtlasS2 |
| Absorption correction | Gaussian (CrysAlis PRO; Rigaku OD, 2015 ▸) |
| T min, T max | 0.097, 0.453 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 18122, 2266, 2242 |
| R int | 0.039 |
| (sin θ/λ)max (Å−1) | 0.633 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.025, 0.066, 1.17 |
| No. of reflections | 2266 |
| No. of parameters | 163 |
| No. of restraints | 10 |
| H-atom treatment | Only H-atom coordinates refined |
| Δρmax, Δρmin (e Å−3) | 0.96, −1.04 |