| Crystal data |
| Chemical formula |
[Mn2Sb2S5(C15H11N3)2]·4H2O |
|
M
r
|
1052.28 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
200 |
|
a, b, c (Å) |
11.9227 (5), 12.1592 (6), 14.9217 (7) |
| α, β, γ (°) |
104.293 (3), 101.701 (3), 112.585 (3) |
|
V (Å3) |
1825.27 (15) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
2.47 |
| Crystal size (mm) |
0.13 × 0.08 × 0.06 |
| |
| Data collection |
| Diffractometer |
Stoe IPDS2
|
| Absorption correction |
Numerical (X-RED and X-SHAPE; Stoe & Cie, 2008 ▸) |
|
T
min, T
max
|
0.624, 0.748 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
7084, 7084, 5834 |
| (sin θ/λ)max (Å−1) |
0.621 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.054, 0.182, 1.07 |
| No. of reflections |
7084 |
| No. of parameters |
444 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.08, −0.98 |
