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. 2020 Jan 1;76(Pt 1):62–65. doi: 10.1107/S2056989019016207

Table 2. Experimental details.

Crystal data
Chemical formula C22H17NO2
M r 327.39
Crystal system, space group Monoclinic, P21/c
Temperature (K) 100
a, b, c (Å) 14.985 (2), 6.0116 (9), 19.106 (3)
β (°) 106.796 (5)
V3) 1647.7 (4)
Z 4
Radiation type Mo Kα
μ (mm−1) 0.09
Crystal size (mm) 0.4 × 0.27 × 0.18
 
Data collection
Diffractometer Bruker APEXII CCD
Absorption correction Multi-scan (SADABS; Krause et al., 2015)
T min, T max 0.629, 0.746
No. of measured, independent and observed [I > 2σ(I)] reflections 25595, 2913, 1975
R int 0.118
(sin θ/λ)max−1) 0.596
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.048, 0.141, 1.12
No. of reflections 2913
No. of parameters 235
H-atom treatment H atoms treated by a mixture of independent and constrained refinement
Δρmax, Δρmin (e Å−3) 0.38, −0.32

Computer programs: APEX2 and SAINT (Bruker, 2016), olex2.solve (Bourhis et al., 2015), olex2.refine (Bourhis et al., 2015), OLEX2 (Dolomanov et al., 2009), Mercury (Macrae et al., 2008), PLATON (Spek, 2009) and publCIF (Westrip, 2010).