Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C22H17NO2 |
| M r | 327.39 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 14.985 (2), 6.0116 (9), 19.106 (3) |
| β (°) | 106.796 (5) |
| V (Å3) | 1647.7 (4) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.09 |
| Crystal size (mm) | 0.4 × 0.27 × 0.18 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.629, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 25595, 2913, 1975 |
| R int | 0.118 |
| (sin θ/λ)max (Å−1) | 0.596 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.048, 0.141, 1.12 |
| No. of reflections | 2913 |
| No. of parameters | 235 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.38, −0.32 |