| Crystal data |
| Chemical formula |
[Cu2(C2H3N)2(C3H6S2)2] (PF6)2
|
|
M
r
|
711.52 |
| Crystal system, space group |
Orthorhombic, P
n
a21
|
| Temperature (K) |
105 |
|
a, b, c (Å) |
11.8409 (9), 12.9273 (9), 15.2921 (11) |
|
V (Å3) |
2340.8 (3) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
2.41 |
| Crystal size (mm) |
0.33 × 0.32 × 0.27 |
| |
| Data collection |
| Diffractometer |
Bruker D8 VENTURE area detector |
| Absorption correction |
Multi-scan (TWINABS; Bruker, 2016 ▸) |
|
T
min, T
max
|
0.608, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
40393, 8122, 7092 |
|
R
int
|
0.040 |
| (sin θ/λ)max (Å−1) |
0.769 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.034, 0.080, 1.03 |
| No. of reflections |
8122 |
| No. of parameters |
293 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.93, −0.73 |
