Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C15H10I2O |
| M r | 460.03 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 200 |
| a, b, c (Å) | 7.2650 (7), 32.864 (3), 5.8446 (6) |
| β (°) | 92.277 (2) |
| V (Å3) | 1394.3 (2) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 4.50 |
| Crystal size (mm) | 0.57 × 0.29 × 0.08 |
| Data collection | |
| Diffractometer | Bruker APEXII kappa CCD area detector |
| Absorption correction | Numerical (SADABS; Bruker, 2016 ▸) |
| T min, T max | 0.065, 0.189 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 18346, 3215, 2960 |
| R int | 0.021 |
| (sin θ/λ)max (Å−1) | 0.650 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.037, 0.073, 1.27 |
| No. of reflections | 3215 |
| No. of parameters | 164 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 1.14, −1.31 |