Table 1.
Volatile composition of two butters using SPME and SDE (n = 3)
| Compounds | RI | RI′ | Thresholds (mg/kg) | SDE | SPME | ||||||
|---|---|---|---|---|---|---|---|---|---|---|---|
| Estimated contents (μg/kg) | OAVs | Estimated contents (μg/kg) | OAVs | ||||||||
| B1 | B2 | B1 | B2 | B1 | B2 | B1 | B2 | ||||
| Methyl ketones | |||||||||||
| 2-Pentanone | 961 | 978a | 61d | 207.72 ± 25.09 | 192.78 ± 9.81 | 0.00 ± 0.00 | 0.00 ± 0.00 | NI | NI | NI | NI |
| 2-Methyl-3-pentanone | 1041 | NA | NA | 21.87 ± 5.84 | NI | NI | NI | NI | NI | NI | NI |
| 2-Hexanone | 1063 | 1046a | NA | 18.53 ± 0.55 | 24.11 ± 0.37** | NI | NI | NI | NI | NI | NI |
| 3-Penten-2-one | 1103 | 1121a | NA | 13.94 ± 0.34 | NI | NI | NI | NI | NI | NI | NI |
| 2-Heptanone | 1170 | 1180a | 15d | 788.56 ± 54.46 | 688.42 ± 41.61 | 0.05 ± 0.00 | 0.05 ± 0.00 | NI | NI | NI | NI |
| 2-Octanone | 1263 | 1283a | 2.5d | NI | 18.74 ± 0.95 | NI | 0.01 ± 0.00 | NI | NI | NI | NI |
| 2-Nonanone | 1371 | 1389a | 7.7d | 526.76 ± 35.23 | 496.72 ± 37.23 | 0.07 ± 0.00 | 0.06 ± 0.00 | 84.10 ± 39.89 | 193.54 ± 11.83 | 0.01 ± 0.01 | 0.03 ± 0.00 |
| 2-Undecanone | 1579 | 1596a | 100d | 400.54 ± 36.26 | 382.68 ± 32.55 | 0.00 ± 0.00 | 0.00 ± 0.00 | NI | NI | NI | NI |
| 2-Tridecanone | 1788 | 1817a | 182d | 401.97 ± 48.82 | 362.97 ± 39.01 | 0.00 ± 0.00 | 0.00 ± 0.00 | NI | NI | NI | NI |
| 2-Pentadecanone | 2000 | 2022b | NA | 464.25 ± 54.24 | 386.08 ± 51.71 | NI | NI | NI | NI | NI | NI |
| In total | 2844.16 | 2552.50 | 84.10 | 193.54 | |||||||
| Lactones | |||||||||||
| δ-Hexalactone | 1737 | NA | 5f | NI | NI | NI | NI | 105.07 ± 44.42 | 152.18 ± 73.78 | 0.02 ± 0.01 | 0.03 ± 0.01 |
| δ-Octanolactone | 1913 | 1902b | 0.1f | NI | NI | NI | NI | 329.35 ± 149.27 | 551.04 ± 238.57 | 3.29 ± 1.49 | 5.51 ± 2.39 |
| δ-Decalactone | 2143 | 2203c | 1f | 40.07 ± 2.97 | 50.69 ± 7.50 | 0.04 ± 0.00 | 0.05 ± 0.00 | 576.37 ± 276.99 | 1122.93 ± 473.60 | 0.58 ± 0.28 | 1.12 ± 0.47 |
| γ-Dodecalactone | 2325 | NA | 1f | NI | 53.05 ± 5.88 | NI | 0.05 ± 0.00 | NI | NI | NI | NI |
| δ-Dodecalactone | 2375 | 2490b | 10f | 102.35 ± 16.86 | 108.35 ± 11.59 | 0.01 ± 0.00 | 0.01 ± 0.00 | 197.18 ± 95.13 | 459.31 ± 314.85 | 0.02 ± 0.01 | 0.05 ± 0.03 |
| δ-Tetradecalactone | 2607 | NA | 50f | 49.11 ± 7.51 | 53.15 ± 5.49 | 0.00 ± 0.00 | 0.00 ± 0.00 | NI | NI | NI | NI |
| In total | 191.53 | 265.24 | 1207.96 | 2285.46 | |||||||
| Fatty acids | |||||||||||
| Butanoic acid | 1586 | 1629b | 0.66d | NI | NI | NI | NI | 268.81 ± 84.52 | 437.55 ± 156.60 | 0.41 ± 0.13 | 0.66 ± 0.24 |
| Hexanoic acid | 1802 | 1856b | 2.50d | NI | NI | NI | NI | 324.58 ± 137.69 | 1037.92 ± 420.6 | 0.13 ± 0.06 | 0.42 ± 0.17 |
| Octanoic acid | 2018 | 2069b | 350d | NI | NI | NI | NI | 655.62 ± 431.29 | 1310.74 ± 694.61 | 0.00 ± 0.00 | 0.00 ± 0.00 |
| Decanoic acid | 2228 | 2282b | 200d | NI | NI | NI | NI | 870.48 ± 526.82 | 1719.04 ± 749.58 | 0.00 ± 0.00 | 0.00 ± 0.00 |
| Dodecanoic acid | 2444 | 2551b | 700d | 40.85 ± 5.03* | 18.43 ± 2.64 | 0.00 ± 0.00 | 0.00 ± 0.00 | 298.63 ± 202.38 | 456.10 ± 212.02 | 0.00 ± 0.00 | 0.00 ± 0.00 |
| Tetradecanoic acid | 2652 | NA | 5000d | 67.00 ± 8.15* | 39.67 ± 1.28 | 0.00 ± 0.00 | 0.00 ± 0.00 | 263.18 ± 103.35 | 295.88 ± 137.04 | 0.00 ± 0.00 | 0.00 ± 0.00 |
| Hexadecanoic acid | 2864 | NA | 10000d | 314.43 ± 33.46* | 227.00 ± 15.33 | 0.00 ± 0.00 | 0.00 ± 0.00 | 710.30 ± 92.69 | 940.17 ± 359.65 | 0.00 ± 0.00 | 0.00 ± 0.00 |
| In total | 422.28 | 285.11 | 3391.60 | 6197.41 | |||||||
| Aldehydes | |||||||||||
| Nonanal | 1373 | 1394a | NA | NI | 20.19 ± 1.82 | NI | NI | 484.79 ± 198.55 | 1392.47 ± 1124.52 | NI | NI |
| Decanal | 1475 | 1495a | 2e | NI | NI | NI | NI | 187.17 ± 72.82 | 356.13 ± 178.10 | 0.09 ± 0.04 | 0.22 ± 0.04 |
| (E)-2-Nonenal | 1505 | 1447a | 45 g | NI | NI | NI | NI | 58.65 ± 26.50 | NI | 0.00 ± 0.00 | NI |
| In total | 201.9 | 730.61 | 1748.60 | ||||||||
| Others | |||||||||||
| Toluene | 1014 | 1035a | NA | NI | NI | NI | NI | 1000.72 ± 451.64 | 458.04 ± 243.77 | NI | NI |
| 1,2-Dutanediol | 1143 | NA | NA | NI | 14.35 ± 3.59 | NI | NI | NI | NI | NI | NI |
| D-Limonene | 1183 | NA | 10e | 30.03 ± 8.81 | 13.89 ± 5.16 | 0.00 ± 0.00 | 0.00 ± 0.00 | NI | NI | NI | NI |
| Styrene | 1230 | NA | NA | NI | 21.29 ± 3.26 | NI | NI | 228.87 ± 77.85 | 579.65 ± 243.13 | NI | NI |
| Ethyl caprylate | 1415 | NA | NA | NI | NI | NI | NI | 75.08 ± 37.99 | NI | NI | NI |
| Furfural | 1423 | 1456a | NA | NI | NI | NI | NI | NI | 84.14 ± 35.48 | NI | NI |
| Benzaldehyde | 1481 | 1515a | NA | NI | NI | NI | NI | 136.08 ± 47.11 | 346.76 ± 119.41 | NI | NI |
| 2-Furanmethanol | 1624 | NA | NA | 50.95 ± 2.22 | 80.43 ± 40.81 | NI | NI | NI | NI | NI | NI |
| 2,4-Dimethyl-benzaldehyde | 1764 | NA | NA | 16.90 ± 5.51 | NI | NI | NI | NI | NI | NI | NI |
| Dimethyl sulfone | 1838 | NA | NA | NI | NI | NI | NI | 181.12 ± 76.35 | 445.04 ± 250.85 | NI | NI |
| Phenol | 1953 | 2051a | NA | NI | NI | NI | NI | 23.79 ± 9.59 | NI | NI | NI |
a–cRIs were mainly gathered from an online database (http://www.odour.org.uk) and the literature (Peterson and Reineccius, 2003b; Wang and Xu, 2009); d–gThreshold values were gathered from literature (Mallia et al., 2007; Urbach et al., 1972) and the online database (http://www.odour.org.uk)
NA, not available; NI, not identified
*p < 0.05; **p < 0.01