Table 1.
Entry | Method | Zein/f-CNOs | Cross-Linker (GA) | Time (min.) | Hydrogel d |
---|---|---|---|---|---|
1. | Conventional | (1.0 g/2.0 mg) | (1%, w/w) | 180 a | CZCNOs |
2. | Microwave | (1.0 g/2.0 mg) | (1%, w/w) | 40 b | MZCNOs |
3. | Acoustic cavitation (ultra-sonic) | (1.0 g/2.0 mg) | (1%, w/w) | 30 c | UZCNOs |
a The reaction mixture was stirred at 65 °C for 180 min; b 500 W of power was applied for 40 min; c The reaction mixture was ultra-sonicated for 30 min; d The homogeneous reaction mixture was poured into a glass petri dish and left to stand overnight for gel formation.