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. 2019 Nov 20;8(12):527. doi: 10.3390/plants8120527

Table 1.

1H and 13C NMR data of compounds 1 and 2 in CD3OD (δ in ppm, 800 MHz for 1H and 200 MHz for 13C) a.

Position 1 2
δ H δ C δ H δ C
1 127.0 127.3
2 7.01 d (1.5) 109.2 7.74 d (2.0) 112.6
3 146.5 145.9
4 147.9 147.0
5 6.89 d (8.0) 114.6 6.86 d (8.0) 113.7
6 7.05 dd (1.5, 8.0) 123.1 7.08 dd (2.0, 8.0) 125.5
7 7.58 d (16.0) 114.6 6.77 d (13.0) 143.7
8 6.27 d (16.0) 115.6 5.79 d (13.0) 116.8
9 167.3 166.7
1′ 4.16 t (7.0) 64.4 4.09 t (7.0) 64.4
2′ 1.37 m 28.6 1.30 m 28.5
3′ 1.67 m 25.9 1.62 m 25.8
4′ n.d.b n.d. b
5′ 1.23 s 29.5 1.23 s 29.5
6′ 1.23 s 29.5 1.23 s 29.5
–OCH3 3.91 s 55.6 3.91 s 55.6

aJ values are in parentheses and reported in Hz; 13C NMR assignments are based on 1H-1H COSY, HSQC, and HMBC experiments; b not detected.