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. 2019 Dec 27;5(1):334–343. doi: 10.1021/acsomega.9b02746

Table 2. Nuclear Magnetic Resonance (NMR) Spectroscopic Data (600 MHz, DMSO) for 5 and 6.

  5 6
position δC δH (J in Hz) δC δH (J in Hz)
1 158.9 14.18, s 158.0  
2 103.4   110.6  
3 157.1   162.4  
4 93.6 6.32, s 104.3  
4a 155.6   152.6  
5 100.0 6.73, s 147.6  
6 152.1 11.18, s 120.6 7.28, dd (7.8, 1.3)
7 141.0 8.69, s 124.0 7.24, t (7.8)
8 129.9   114.6 7.55, dd (7.8, 1.3)
8a 110.1   120.3  
9 181.7   180.8  
9a 102.9   102.2  
10a 152.8   146.5  
11 114.8 6.60, d (10.0) 21.4 3.28, d (7.0)
12 127.8 5.72, d (10.0) 122.4 5.18, d (7.4)
13 77.9   130.8  
14 29.1 1.20, s 25.6 1.61, s
15 29.1 1.20, s 17.9 1.67, s
16 43.6 1.57, m 29.2 3.21, dd (14.7, 3.2), 3.03, dd (14.8, 7.7)
17 21.9 3.30, dd (9.7, 6.8) 74.6 4.32, m
18 69.3 1.3, s 144.9  
19 27.9 1.42, s 109.8 4.86, s; 4.72, s
20 27.9 1.42, s 18.5 1.81, s