Table 1.
Data collection and refinement statistics (molecular replacement)
| Data collection | |
| Space group | I222 |
| Cell dimensions | |
| a, b, c, Å | 106.97 130.60 131.79 |
| α, β, γ, ° | 90.00 90.00 90.00 |
| Resolution, Å | 30–2.80 (2.91–2.80)* |
| Rsym or Rmerge | 0.07 (0.99) |
| I/σI | 21.42 (1.93) |
| Completeness, % | 98 (100) |
| Redundancy | 6.1 (6.2) |
| CC1/2 | 0.72 |
| Refinement | |
| Resolution, Å | 32.85–2.80 (2.93–2.80) |
| No. reflections | 23,040 (2,836) |
| Rwork/Rfree | 0.24/0.27 |
| No. atoms in an AU | 4,178 |
| Protein | 4,178 |
| Ligand/ion | 0 |
| Water | 0 |
| B factors | |
| Protein | 107.9 |
| Ligand/ion | |
| Water | |
| R.m.s. deviations | |
| Bond lengths, Å | 0.004 |
| Bond angles, ° | 0.685 |
*
Values in parentheses are for highest-resolution shell.