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. 2019 Jun 22;27(7):920–929. doi: 10.1016/j.jsps.2019.06.006

Table 1.

Selected 1H NMR data (δ ppm, J in parenthese in Hz) for compounds 13, 5 and 6.

Pos 1 2 3 5 6
2 7.11 (d, J = 7.5) 7.32 (d, J = 8.3) 7.45 (d, J = 8.4) 7.48 (d, J = 8.4)
3 6.92
(dd, J = 1.5, 7.5)
7.90, m 7.00, m 7.00, m
5 7.01 (d, J = 1.5) 7.90, m 5.44 (d, J = 4.4) 7.00, m 7.00, m
7 2.68, m 1.16, m 2.58, m 2.68, m
11 2.22, m 3.71, m 1.96, m 1.99, m 2.01, m
12 0.71 (d, J = 7.0) 1.37 (d, J = 6.8) 0.80 (d, J = 7.0) 0.76 (d, J = 6.9) 0.70 (d, J = 6.6)
13 0.99 (d, J = 7.0) 1.37 (d, J = 6.8) 0.87 (d, J = 7.0) 1.04 (d, J = 6.9) 1.02 (d, J = 6.6)
14 1.24 (d, J = 6.7) 2.63, s 0.96 (d, J = 6.6) 1.51, s 1.48, s
15 2.28, s 2.54, s 1.70, s 2.95, s 2.30, s

1: 2.74 (m, H-10); 2: 7.19 (d, J = 8.0, H-8), 7.25 (d, J = 8.0, H-8); 5: 1.58 (m, H-10); 6: 1.69 (m, H-6).