Table 1.
Pos | 1 | 2 | 3 | 5 | 6 |
---|---|---|---|---|---|
2 | 7.11 (d, J = 7.5) | 7.32 (d, J = 8.3) | 7.45 (d, J = 8.4) | 7.48 (d, J = 8.4) | |
3 | 6.92 (dd, J = 1.5, 7.5) |
7.90, m | 7.00, m | 7.00, m | |
5 | 7.01 (d, J = 1.5) | 7.90, m | 5.44 (d, J = 4.4) | 7.00, m | 7.00, m |
7 | 2.68, m | – | 1.16, m | 2.58, m | 2.68, m |
11 | 2.22, m | 3.71, m | 1.96, m | 1.99, m | 2.01, m |
12 | 0.71 (d, J = 7.0) | 1.37 (d, J = 6.8) | 0.80 (d, J = 7.0) | 0.76 (d, J = 6.9) | 0.70 (d, J = 6.6) |
13 | 0.99 (d, J = 7.0) | 1.37 (d, J = 6.8) | 0.87 (d, J = 7.0) | 1.04 (d, J = 6.9) | 1.02 (d, J = 6.6) |
14 | 1.24 (d, J = 6.7) | 2.63, s | 0.96 (d, J = 6.6) | 1.51, s | 1.48, s |
15 | 2.28, s | 2.54, s | 1.70, s | 2.95, s | 2.30, s |
1: 2.74 (m, H-10); 2: 7.19 (d, J = 8.0, H-8), 7.25 (d, J = 8.0, H-8); 5: 1.58 (m, H-10); 6: 1.69 (m, H-6).