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. 2019 Jun 22;27(7):920–929. doi: 10.1016/j.jsps.2019.06.006

Table 2.

Selected 1H NMR data (δ ppm, J in parenthese in Hz) for compounds 4 and 79.

Pos 4 7 8 9
7 5.43, bs 5.31 (d, J = 4.3) 5.22, s
14 5.91
(dd, J = 10.75, 17.35)
5.78
15 5.04 (d, J = 10.75)
5.20 (d, J = 17.35)
5.81
(dd, J = 10.5, 17.5)
5.77
(dd, J = 10.2, 17.0)
16 1.26 s 0.99 J = 5.0 4.86 d J = 10.5
4.92 d J = 17.5
4.84 (d, J = 10.2)
4.90 (d, J = 17.0)
17 4.48, s
4.80, s
1.02 (d, J = 5.0) 0.86, s 0.83, s
18 0.87, s 1.25, s 1.26, s 1.19, s
19 0.80, s
20 0.67, s 0.71, s 0.90, s 1.04, s