Fig. 2. Size comparisons of HKUST-1 nanocrystals prepared by (A) microwave-assisted growth at varying reactant concentrations and added equivalents of dodecanoic acid and (B) by solvothermal synthesis at a fixed reactant concentration of 0.0024 M and varying equivalents of triethylamine (TEA) or acetate (OAc) modulators.44,86,87 The nanocrystal sizes in these studies were determined by TEM (A) and PXRD (B).
