Table 3.
Recovery and accuracy results for determining nine sweeteners in three different spirit samples.
| Analytes | Added (μg/g) | White Spirits 38° | White Spirits 46° | White Spirits 52° | ||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Found | Recovery | RSD | Found | Recovery | RSD | Found | Recovery | RSD | ||
| ACS-K | 5.0 | 4.88 | 97.6% | 3.0% | 4.74 | 94.8% | 2.8% | 4.80 | 96.0% | 2.5% |
| 10.0 | 9.59 | 95.9% | 3.2% | 9.67 | 96.7% | 2.7% | 9.71 | 97.1% | 2.2% | |
| 40.0 | 38.49 | 96.2% | 2.9% | 38.18 | 95.4% | 2.5% | 39.04 | 97.6% | 2.1% | |
| CYC | 5.0 | 5.23 | 104.5% | 3.6% | 5.12 | 102.5% | 3.4% | 5.25 | 104.9% | 2.9% |
| 10.0 | 10.20 | 102.0% | 3.8% | 10.28 | 102.8% | 3.2% | 10.21 | 102.1% | 3.0% | |
| 40.0 | 40.32 | 100.8% | 3.1% | 41.15 | 102.9% | 2.9% | 41.56 | 103.9% | 2.6% | |
| SAC | 5.0 | 4.80 | 96.0% | 3.1% | 4.76 | 95.1% | 2.8% | 4.78 | 95.5% | 2.3% |
| 10.0 | 9.63 | 96.3% | 3.0% | 9.78 | 97.8% | 2.6% | 9.69 | 96.9% | 2.2% | |
| 40.0 | 39.64 | 99.1% | 3.3% | 40.33 | 100.8% | 3.0% | 40.25 | 100.6% | 2.3% | |
| SCL | 5.0 | 4.99 | 99.8% | 2.9% | 5.04 | 100.8% | 2.2% | 4.98 | 99.5% | 2.3% |
| 10.0 | 9.96 | 99.6% | 2.7% | 10.02 | 100.2% | 2.8% | 9.95 | 99.5% | 2.6% | |
| 40.0 | 40.33 | 100.8% | 3.1% | 39.88 | 99.7% | 2.7% | 39.67 | 99.2% | 2.4% | |
| ASP | 5.0 | 4.98 | 99.7% | 2.8% | 5.13 | 102.6% | 2.3% | 4.90 | 98.1% | 1.6% |
| 10.0 | 9.97 | 99.7% | 2.5% | 9.81 | 98.1% | 2.4% | 9.89 | 98.9% | 1.9% | |
| 40.0 | 39.00 | 97.5% | 2.7% | 38.62 | 96.5% | 2.4% | 39.24 | 98.1% | 2.0% | |
| DUL | 5.0 | 4.86 | 97.1% | 3.3% | 4.72 | 94.3% | 2.3% | 4.82 | 96.3% | 2.7% |
| 10.0 | 10.01 | 100.1% | 3.0% | 9.82 | 98.2% | 2.9% | 9.62 | 96.2% | 2.6% | |
| 40.0 | 38.56 | 98.4% | 3.2% | 38.80 | 97.0% | 2.8% | 39.93 | 99.8% | 2.4% | |
| ALI | 5.0 | 4.79 | 98.8% | 3.3% | 4.76 | 98.2% | 3.0% | 4.76 | 97.2% | 2.4% |
| 10.0 | 9.90 | 96.0% | 3.1% | 9.97 | 97.7% | 2.6% | 9.77 | 97.7% | 1.9% | |
| 40.0 | 38.76 | 97.0% | 3.4% | 39.07 | 97.7% | 2.9% | 38.88 | 97.3% | 2.3% | |
| NHDC | 5.0 | 4.89 | 97.8% | 3.1% | 4.81 | 96.2% | 2.2% | 4.90 | 98.1% | 1.9% |
| 10.0 | 9.88 | 98.8% | 3.0% | 9.97 | 99.7% | 2.5% | 9.93 | 99.3% | 2.2% | |
| 40.0 | 39.39 | 98.5% | 3.3% | 39.01 | 97.5% | 2.6% | 39.08 | 97.7% | 2.3% | |
| NEO | 5.0 | 4.91 | 98.2% | 2.9% | 4.79 | 95.9% | 2.6% | 4.96 | 99.1% | 1.8% |
| 10.0 | 9.69 | 96.9% | 3.3% | 9.81 | 98.1% | 2.7% | 9.82 | 98.2% | 2.1% | |
| 40.0 | 38.51 | 96.3% | 3.0% | 38.74 | 96.9% | 2.8% | 38.71 | 96.8% | 2.3% | |